Details of experiments between P98088 and O00499
Note that the results of all experiments are listed, regardless of the modification states of the fragments.



Experiment series 1

Protein A protein: MUC5AC
Protein A fragment: 1-5654
Protein A construct: endogenous protein (Jurkat)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.9
Immobilized partner concentration in holdup experiment (10-6M): 10
P value (usually -log10(P Two-sided unpaired T-test), but double check the experimental details): 0.72
Experiment method: nHU_Jurkat
Details of affinity fitting: hyperbolic binding equation
Date of measurement: 2022.06.29.
Experimental details: -log10(P Two-sided unpaired T-test (6 vs 3))
Number of measurements: 3
The affinity was below the detection threshold of the assay.


Experiment series 2

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0
Holdup BI standard deviation: 0.01
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 3

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.06
Holdup BI standard deviation: 0.04
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
Measured pKd: 3.54


Experiment series 4

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.02
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 5

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0.03
Holdup BI standard deviation: 0.09
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 6

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0
Holdup BI standard deviation: 0.01
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 7

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.01
Holdup BI standard deviation: 0.06
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 8

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.01
Holdup BI standard deviation: 0.04
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 9

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0.04
Holdup BI standard deviation: 0.11
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.06.29.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 10

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: D537V
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0.06
Holdup BI standard deviation: 0.06
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 11

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: D537V
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.03
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 12

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: D537V
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.02
Holdup BI standard deviation: 0.02
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 13

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: D537V
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.03
Holdup BI standard deviation: 0.07
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 14

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: F584S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.01
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 15

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: F584S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.08
Holdup BI standard deviation: 0.08
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 3.66


Experiment series 16

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: F584S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.03
Holdup BI standard deviation: 0.06
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 17

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: F584S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.09
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 18

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: P551L
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.02
Holdup BI standard deviation: 0
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 19

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: P551L
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.02
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 20

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: P551L
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.02
Holdup BI standard deviation: 0.09
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 21

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: P551L
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.06
Holdup BI standard deviation: 0.07
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 4.05


Experiment series 22

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Q540H
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0.08
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 23

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Q540H
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.01
Holdup BI standard deviation: 0.05
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 24

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Q540H
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.07
Holdup BI standard deviation: 0.06
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 3.66


Experiment series 25

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Q540H
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.06
Holdup BI standard deviation: 0.07
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 3.58


Experiment series 26

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0.01
Holdup BI standard deviation: 0.01
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 27

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 28

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.05
Holdup BI standard deviation: 0.04
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 29

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: T532M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.05
Holdup BI standard deviation: 0.05
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 3.5


Experiment series 30

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V566M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 31

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V566M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.05
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 32

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V566M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.05
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 33

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V566M
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.08
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 34

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V583I
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0.03
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 9
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 35

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V583I
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.03
Holdup BI standard deviation: 0.07
Immobilized partner concentration in holdup experiment (10-6M): 9
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 36

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V583I
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.02
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 9
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 37

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: V583I
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.12
Immobilized partner concentration in holdup experiment (10-6M): 9
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 38

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.01
Holdup BI standard deviation: 0.01
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 39

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.03
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 40

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: -0
Holdup BI standard deviation: 0.02
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 41

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.05
Holdup BI standard deviation: 0.11
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 42

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Y531S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.01
Holdup BI standard deviation: 0.01
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 43

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Y531S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.05
Holdup BI standard deviation: 0.06
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 44

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Y531S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 45

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: Y531S
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.05
Holdup BI standard deviation: 0.11
Immobilized partner concentration in holdup experiment (10-6M): 18
Experiment method: HU (DAPF)
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 3.5


Experiment series 46

Protein A protein: MUC5AC
Protein A fragment: 1311-1325
Protein A site: PxxP_1
Protein A sequence: IERRVYPCSPTTPVP
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: R581C
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0
Holdup BI standard deviation: 0.03
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 47

Protein A protein: MUC5AC
Protein A fragment: 1563-1577
Protein A site: PxxP_2
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: R581C
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.02
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 48

Protein A protein: MUC5AC
Protein A fragment: 1936-1950
Protein A site: PxxP_3
Protein A sequence: VSSKPTPTEPSTSSC
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: R581C
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.04
Holdup BI standard deviation: 0.02
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
The affinity was below the detection threshold of the assay.


Experiment series 49

Protein A protein: MUC5AC
Protein A fragment: 5643-5657
Protein A site: PxxP_4
Protein A sequence: SWERGVPVSPMH---
Protein A construct: Biotinylated 15-mer peptide (crude)

Protein B protein: BIN1
Protein B fragment: 513-593
Protein B site: SH3
Protein B modification: R581C
Protein B construct: avi(biotin)-his6-MBP-TEVsite-SH3

Average holdup BI: 0.06
Holdup BI standard deviation: 0.09
Immobilized partner concentration in holdup experiment (10-6M): 6
Experiment method: HU (DAPF)
Details of affinity fitting: Bait concentration was adjusted to fit the profile to WT
Date of measurement: 2022.10.24.
Number of measurements: 2
Measured pKd: 4.03